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Analytical Column Articles & Analysis

45 articles found

LC6000 Good Practice Handbook

LC6000 Good Practice Handbook

Poor pH control can lead to damage of the LC6000 and analytical column. When using a buffered mobile phase, always use a plunger wash on the 6100 Pump as this will eliminate the build-up of any salts within the buffer. ...

BySCION Instruments BV - Techcomp Group


Determination of Aromatic Hydrocarbons in Diesel Fuel by LC-RID According to ASTM D6591

Determination of Aromatic Hydrocarbons in Diesel Fuel by LC-RID According to ASTM D6591

Due to the use of a 3 micrometer packing analytical column, the instrument is also in compliance with ASTM D6379 for jet fuel, kerosene, and middle distillates with boiling points in the range of 50° to 300° C without change to the instrument ...

ByShimadzu Scientific Instruments Inc


How does an FID work?

How does an FID work?

An FID, or Flame Ionization Detector, is the most common detector paired with gas chromatography instruments for analytical applications. But how does and FID work? An FID uses a flame to ionize organic compounds containing carbon. Following separation of the sample in the GC column, each analyte passes through a flame, fuelled by hydrogen ...

ByPEAK Scientific Instruments Ltd


Development of on-line instruments for monitoring of methane and NMTHC at PPB and PPM levels without matrix effects

Development of on-line instruments for monitoring of methane and NMTHC at PPB and PPM levels without matrix effects

For this study, a Gas Chromatograph (GC) with two analytical columns and a Flame Ionization Detector (FID) is used to achieve the absolute separation of methane, NMTHC and matrix gases. ...

ByChromatotec


Troubleshooting injection volume variation in the Concurrent Solvent Recondensation – Large Volume Sample Injection Technique

Troubleshooting injection volume variation in the Concurrent Solvent Recondensation – Large Volume Sample Injection Technique

Early runs collected under the final GC analytical conditions showed great retention time variation for these compounds. ...

ByRestek Corporation


Update on Guard Cartridges for Trident Holders

Update on Guard Cartridges for Trident Holders

You may have seen my last blog post about guard holders and cartridges that we have available for our various LC product lines, “Which guard cartridges and holders go with which LC analytical columns?” Along those lines of discussion, the following note is available to also show what specific products are currently offered for this: ...

ByRestek Corporation


Two Detector Solution to Analyzing Sulfur

Two Detector Solution to Analyzing Sulfur

The injection volume was 1 mL. The GC analytical column was a 15 m × 0.25 mm × 0.25 µm Rtx-1 (Cat # 10120). A three-port SilFlow device (SGC Analytical Science) was employed to split the flow at the end of analytical column to both MS and FPD. ...

ByRestek Corporation


The productive environmental laboratory: BSK Labs boosts efficiency with Metrohm IC

The productive environmental laboratory: BSK Labs boosts efficiency with Metrohm IC

Fully automated Inline Ultrafiltration protects the separation column – and the budget At BSK Labs, all samples are filtered before being analyzed. ...

ByMetrohm AG


Method Scaling in Preparative HPLC:  Analytical Method & Preparative Method

Method Scaling in Preparative HPLC: Analytical Method & Preparative Method

Ensure that a preparative version of your analytical column is available because your column chemistry needs to be the same. ...

ByWaters Corporation


Fast analysis of semi-volatile organic compounds using PTV-GC–TOF MS

Fast analysis of semi-volatile organic compounds using PTV-GC–TOF MS

The evaluation of semi-volatile organic compounds (SVOCs) in environmental matrices poses many challenges for the analyst, not least the vast number that may be encountered in any given analysis. In addition, analyte reactivity and the potential for multiple analytes to co-elute makes achieving the required method detection limits (LODs or MDLs) quickly and ...

BySepSolve Analytical - a company of the Schauenburg International Group


What is microflow?

What is microflow?

Compared to the conventional flow, the microflow approach downsizes two key variables: (1) the inner diameter (ID) of the fluidic channel inside the separation device, for example, the LC column; (2) the volume of fluid flowing through the columns in a given time. ...

ByWaters Corporation


High-throughput Microscale Bioanalysis is not a Paradox

High-throughput Microscale Bioanalysis is not a Paradox

This is comparable to the 2- to 4-minute total gradient/cycle time of traditional throughput workflows on wide-bore columns at analytical scale. Did Dr. Alelyunas use pixie dust or a magic wand? ...

ByWaters Corporation


Interactions of Haptoglobin with Monomeric Globin Species: Insights from Molecular Modeling and Native Electrospray Ionization Mass Spectrometry

Interactions of Haptoglobin with Monomeric Globin Species: Insights from Molecular Modeling and Native Electrospray Ionization Mass Spectrometry

Mb is homologous to both the α- and β-chains of Hb and shares many conserved Hb/Hp interface residues, yet whether Hp binds Mb remains unclear…Hb α- and β-chains were separated via reversed phase high-performance liquid chromatography…using a 4.6 mm × 150 mm C8 [O-5-100/15] analytical column with a 5 μm pore size ...

BySeparation Methods Technologies, Inc. (SMT)


Surface Decontamination of Alkaloids (Nicotine) by DeconGel 1101

Surface Decontamination of Alkaloids (Nicotine) by DeconGel 1101

Decontamination efficacies of DeconGel 1101 were from 99.5% (on concrete) to 99.8% (on aluminum) to 99.8% (on stainless steel) for Nicotine determined by residual swipe analysis. Optimized experimental and analytical methods were successfully developed following standardized EPA sampling and analysis methods as guidelines for determination of organic compounds dissolved in a ...

ByIndustrial Chem Solutions, Inc. is a subsidiary of Worldwide Specialty Chemicals, Inc.


Surface Decontamination of Aromatic Liquids (Toluene) by DeconGel 1101 and 1102

Surface Decontamination of Aromatic Liquids (Toluene) by DeconGel 1101 and 1102

Decontamination efficacies of poured DeconGel 1102 ranged from 100% (on concrete) to 100% (on floor tile) to 100% (on stainless steel), brushed DeconGel 1102 ranged from 100% (on concrete) to 100% (on floor tile) to 100% (on stainless steel), as determined by residual swipe analysis. Optimized experimental and analytical methods were successfully developed following standardized ...

ByIndustrial Chem Solutions, Inc. is a subsidiary of Worldwide Specialty Chemicals, Inc.


Surface Decontamination of Aromatic Solids (Naphthalene) by DeconGel 1101

Surface Decontamination of Aromatic Solids (Naphthalene) by DeconGel 1101

Decontamination efficacies of DeconGel 1101 ranged from 99.2% (on concrete) to 99.6% (on stainless steel) to 99.2% (on aluminum) for Naphthalene as determined by residual swipe analysis. Optimized experimental and analytical methods were successfully developed following standardized EPA sampling and analysis methods as guidelines for determination of organic compounds dissolved ...

ByIndustrial Chem Solutions, Inc. is a subsidiary of Worldwide Specialty Chemicals, Inc.


Surface Decontamination of Industrial Coolants (Ethylene Glycol) by DeconGel 1101

Surface Decontamination of Industrial Coolants (Ethylene Glycol) by DeconGel 1101

Decontamination efficacies of DeconGel 1101 ranged from 93.6% (on concrete) to 95.5% (on stainless steel) to 95.5% (on aluminum) for EG determined by residual swipe analysis. Optimized experimental and analytical methods were successfully developed following standardized EPA sampling and analysis methods as guidelines for determination of organic compounds dissolved in a ...

ByIndustrial Chem Solutions, Inc. is a subsidiary of Worldwide Specialty Chemicals, Inc.


Surface Decontamination of Hydrocarbon Petroleum Distillates (Kerosene) by DeconGel 1101 and 1102

Surface Decontamination of Hydrocarbon Petroleum Distillates (Kerosene) by DeconGel 1101 and 1102

Decontamination efficacies of poured DeconGel 1102 ranged from 100% (on concrete) to 100% (on aluminum) to 100% (on stainless steel), brushed DeconGel 1102 ranged from 100% (on concrete) to 100% (on aluminum) to 100% (on stainless steel), as determined by residual swipe analysis. Optimized experimental and analytical methods were successfully developed following standardized EPA ...

ByIndustrial Chem Solutions, Inc. is a subsidiary of Worldwide Specialty Chemicals, Inc.


Surface Decontamination of Organic Acids (Benzoic Acid) by DeconGel 1101

Surface Decontamination of Organic Acids (Benzoic Acid) by DeconGel 1101

Decontamination efficacies of DeconGel 1101 ranged from 98.4% (on concrete) to 99.7% (on stainless steel) to 99.8% (on aluminum) for BA determined by residual swipe analysis. Optimized experimental and analytical methods were successfully developed following standardized EPA sampling and analysis methods as guidelines for determination of organic compounds dissolved in a ...

ByIndustrial Chem Solutions, Inc. is a subsidiary of Worldwide Specialty Chemicals, Inc.


Surface Decontamination of Organic Bases (Triethylamine) by DeconGel 1101

Surface Decontamination of Organic Bases (Triethylamine) by DeconGel 1101

Decontamination efficacies of DeconGel 1101 ranged from 99.7% (on concrete) to 99.9% (on stainless steel) to 99.9% (on aluminum) for TEA as determined by residual swipe analysis. Optimized experimental and analytical methods were successfully developed following standardized EPA sampling and analysis methods as guidelines for determination of organic compounds dissolved in a ...

ByIndustrial Chem Solutions, Inc. is a subsidiary of Worldwide Specialty Chemicals, Inc.

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