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Diffuse Reflectance Spectroscopy Articles & Analysis

21 articles found

Best practice methods for reliable results from your DRIFTS setup

Best practice methods for reliable results from your DRIFTS setup

Diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS) is a powerful analytical technique for the study of powdered and rough surface materials. ...

BySpecac


Reverse water-gas shift innovation through DRIFTS: petrochemicals and beyond

Reverse water-gas shift innovation through DRIFTS: petrochemicals and beyond

Researchers and engineers have long searched for viable solutions, and recent progress in reverse water-gas shift (RWGS) catalysis and advanced diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS) now promises to make that vision a reality. ...

BySpecac


What gas can i use for ftir?

What gas can i use for ftir?

Fourier Transform Infrared (FTIR) - spectroscopy is used typically in testing laboratories for understanding materials and products. Fourier Transform Infrared (FTIR) - spectroscopy is used typically in testing laboratories for understanding materials and products, identifying chemical compounds in solids, liquids and gases, consumer products, paints, polymers, ...

ByPEAK Scientific Instruments Ltd


A research on shape-controllable synthesis of Ag3PO4/AgBr and its degradation of ciprofloxacin

A research on shape-controllable synthesis of Ag3PO4/AgBr and its degradation of ciprofloxacin

The as-prepared Ag3PO4/AgBr microspheres were characterized by means of powder X-ray diffraction (XRD), scanning electron microscope (SEM) and UV-visible diffuse reflectance spectroscopy (UV-vis DRS). The results revealed that the Ag3PO4/AgBr sample (synthesized with CTAB, 0.8 g) exhibited the highest photocatalytic activity to the ...

ByIWA Publishing


Optimization of operational variables and kinetic modeling for photocatalytic removal of Direct Blue 14 from aqueous media by ZnS nanoparticles

Optimization of operational variables and kinetic modeling for photocatalytic removal of Direct Blue 14 from aqueous media by ZnS nanoparticles

Zinc sulfide nanoparticles (ZnS-NPs) were synthesized via a simple and facile co-precipitation method and were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and diffuse reflectance spectroscopy (DRS). Photocatalytic activity of synthesized nanoparticles was evaluated in removal of double azo ...

ByIWA Publishing


Synthesis of coral-globular-like composite Ag/TiO2-SnO2 and its photocatalytic degradation of rhodamine B under multiple modes

Synthesis of coral-globular-like composite Ag/TiO2-SnO2 and its photocatalytic degradation of rhodamine B under multiple modes

X-ray diffraction, scanning electron microscopy (SEM), UV–vis diffuse reflectance spectroscopy, X-ray photoelectron spectroscopy, SEM combined with X-ray energy dispersive spectroscopy, and N2 adsorption–desorption tests were employed to characterize samples' crystalline phase, chemical composition, morphology ...

ByIWA Publishing


Preparation of Fe3O4/TiO2 magnetic mesoporous composites for photocatalytic degradation of organic pollutants

Preparation of Fe3O4/TiO2 magnetic mesoporous composites for photocatalytic degradation of organic pollutants

The as-prepared Fe3O4/TiO2 composites were characterized by X-ray diffraction, diffuse reflectance spectroscopy, nitrogen adsorption-desorption isotherm and pore size distribution. ...

ByIWA Publishing


Effect of W doping level on TiO2 on the photocatalytic degradation of Diuron

Effect of W doping level on TiO2 on the photocatalytic degradation of Diuron

The powders obtained were characterized by X-ray diffraction, Raman spectroscopy and UV–visible diffuse reflectance spectroscopy. The photocatalytic performances of the different photocatalysts are tested with respect to the degradation of Diuron in water solutions under simulated solar light and visible light irradiation. ...

ByIWA Publishing


Facile synthesis of TiO2-RGO composite with enhanced performance for the photocatalytic mineralization of organic pollutants

Facile synthesis of TiO2-RGO composite with enhanced performance for the photocatalytic mineralization of organic pollutants

X-ray diffraction (XRD), transmission electron microscopy (TEM), thermogravimetric analysis (TGA), Brunauer–Emmett–Teller surface area (BET), Raman and diffuse reflectance spectroscopy (DRS) technique confirming successful formation of nanocomposite. ...

ByIWA Publishing


Enhanced photocatalytic activity of nanocomposites of TiO2 doped with Zr, Y or Ce polyoxometalates for degradation of methyl orange dye

Enhanced photocatalytic activity of nanocomposites of TiO2 doped with Zr, Y or Ce polyoxometalates for degradation of methyl orange dye

The morphology and crystal phase of the as-prepared nanocomposites were investigated by various characterization techniques: Fourier transform infrared spectroscopy, scanning electron microscopy, transmission electron microscopy, X-ray diffraction, energy-dispersive X-ray analysis and diffuse reflectance spectroscopy, indicating ...

ByIWA Publishing


Industrial and agroindustrial wastes: an echotechnological approach to the production of supported photocatalysts

Industrial and agroindustrial wastes: an echotechnological approach to the production of supported photocatalysts

The solids were characterized by scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM-EDX), diffuse reflectance spectroscopy over the ultraviolet range (DRS-UV), X-ray diffraction (XRD), small-angle X-ray scattering (SAXS), nitrogen adsorption–desorption at −196 °C and zeta potential (ZP) measurements. ...

ByIWA Publishing


Photocatalytic removal of 2-nitrophenol using silver and sulfur co-doped TiO<sub>2</sub> under natural solar light

Photocatalytic removal of 2-nitrophenol using silver and sulfur co-doped TiO<sub>2</sub> under natural solar light

Effects of the co-doping on the structural, optical and morphological properties of the synthesized nanoparticles were investigated by different characterization methods: X-ray diffraction, N2 adsorption–desorption measurements, scanning electron microscopy, transmission electron microscopy, energy-dispersive X-ray spectroscopy, UV–visible diffuse ...

ByIWA Publishing


Enhanced photobactericidal activity of ZnO nanorods modified by meso-tetrakis(4-sulfonatophenyl)porphyrin under visible LED lamp irradiation

Enhanced photobactericidal activity of ZnO nanorods modified by meso-tetrakis(4-sulfonatophenyl)porphyrin under visible LED lamp irradiation

The samples were characterized by various techniques such as X-ray diffraction, diffuse reflectance spectra, Fourier transform-infrared spectroscopy and scanning electron microscopy. ...

ByIWA Publishing


Optimized photocatalytic degradation of caffeic acid by sol&#x2013;gel TiO<sub>2</sub>

Optimized photocatalytic degradation of caffeic acid by sol&#x2013;gel TiO<sub>2</sub>

The characterization of the samples synthesized was complemented by scanning electron microscopy, diffuse reflectance infrared Fourier transform spectroscopy, nitrogen adsorption–desorption isotherms (Brunauer–Emmett–Teller) and diffuse reflectance spectroscopy. ...

ByIWA Publishing


Gemas: Prediction of solid‐solution phase partitioning coefficients (Kd) for oxoanions and boric acid in soils using mid‐infrared diffuse reflectance spectroscopy

Gemas: Prediction of solid‐solution phase partitioning coefficients (Kd) for oxoanions and boric acid in soils using mid‐infrared diffuse reflectance spectroscopy

The authors' aim was to develop rapid and inexpensive regression models for the prediction of partitioning coefficients (Kd), defined as the ratio of the total or surface‐bound metal/metalloid concentration of the solid phase to the total concentration in the solution phase. Values of Kd were measured for boric acid (B(OH)30) and selected added soluble oxoanions: molybdate (MoO42‐), antimonate ...

ByJohn Wiley & Sons, Ltd.


Prediction of solid‐solution partitioning coefficients (Kd) for cationic metals in soils using mid‐infrared diffuse reflectance spectroscopy

Prediction of solid‐solution partitioning coefficients (Kd) for cationic metals in soils using mid‐infrared diffuse reflectance spectroscopy

Partial least squares regression (PLSR) models, using mid‐infrared (MIR) diffuse reflectance Fourier transformed (DRIFT) spectra, were used to predict distribution coefficient (Kd) values for selected added soluble metal cations (Ag+, Co2+, Cu2+, Mn2+, Ni2+, Pb2+, Sn4+, and Zn2+) in 4813 soils of the Geochemical Mapping of Agricultural Soils (GEMAS) program. For the development of the PLSR ...

ByJohn Wiley & Sons, Ltd.


Removal of toluene from water by photocatalytic oxidation with activated carbon supported Fe<sup>3&#x002B;</sup>-doped TiO<sub>2</sub> nanotubes

Removal of toluene from water by photocatalytic oxidation with activated carbon supported Fe<sup>3&#x002B;</sup>-doped TiO<sub>2</sub> nanotubes

The catalyst was used to effectively decompose toluene in water under O3/UV conditions, and some properties including the morphology, X-ray photoelectron spectroscopy, X-ray diffraction patterns, specific surface area and UV-visible diffuse reflectance spectroscopy were analyzed. ...

ByIWA Publishing


Novel catalytic and mechanistic studies on wastewater denitrification with hydrogen

Novel catalytic and mechanistic studies on wastewater denitrification with hydrogen

Steady-state isotopic transient kinetic analysis (SSITKA) experiments coupled with ex situ diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS) were performed on supported Pd-Cu catalysts for the NO3−/H2 and NO3−/H2/O2 reactions. ...

ByIWA Publishing


Preparation of N-doped TiO<sub>2</sub> by oxidizing TiN and its application on phenol degradation

Preparation of N-doped TiO<sub>2</sub> by oxidizing TiN and its application on phenol degradation

The as-prepared samples were characterized by X-ray diffraction, UV-Vis diffuse reflectance spectra and X-ray photoelectron spectroscopy. The results confirmed that oxidizing TiN incompletely is an effective and simple method to prepare nitrogen-doped TiO2. ...

ByIWA Publishing


Catalyst characterisation of Fe-doped-titanium dioxide

Catalyst characterisation of Fe-doped-titanium dioxide

This material was characterised by X-Ray diffraction (XRD), Raman spectroscopy, scanning electron microscope (SEM) imaging, BET surface area, X-Ray photoelectron spectroscopy (XPS) and ultraviolet-visible diffuse reflectance spectroscopy (UV-vis DRS). ...

ByInderscience Publishers

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