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Headspace Vial Articles & Analysis

19 articles found

A Novel Analysis of Solvent Residual in Cannabis Oil Using Dynamic Headspace by PAL System

A Novel Analysis of Solvent Residual in Cannabis Oil Using Dynamic Headspace by PAL System

In the USP 467 method, the dynamic headspace technique was used as the Gas Chromatography (GC) sample introduction method. ...

ByCDS Analytical


Flavor and Aroma Profile of Hops Using FET-Headspace on the Teledyne Tekmar Versa with GC/MS

Flavor and Aroma Profile of Hops Using FET-Headspace on the Teledyne Tekmar Versa with GC/MS

In this application note, the flavor profile of five types of hops will be identified using Full Evaporation Technique (FET) Headspace on a Teledyne Tekmar Versa Automated Headspace vial sampler connected to a GC/MS (Gas Chromatograph/Mass Spectrometer) for chromatographic separation and detection. ...

ByTeledyne Tekmar


Meeting the Korean Method ES 04605.3 for Formaldehyde with Static Headspace GC/MS

Meeting the Korean Method ES 04605.3 for Formaldehyde with Static Headspace GC/MS

Introduction The Korean Standard Method for Drinking Water ES 04605.3 requires static headspace with Gas Chromatograph/Mass Spectrometer (GC/MS) to monitor formaldehyde. The method is based on the derivatization of formaldehyde with O-(2,3,4,5,6-pentafluorobenzyl) hydroxylamine (PFBHA) to form the pentafluorobenzyl oximine compound within a static headspace ...

ByTeledyne Tekmar


Meeting the Korean Method ES 04607.1 for Naphthalene with Static and Dynamic Headspace GC/MS

Meeting the Korean Method ES 04607.1 for Naphthalene with Static and Dynamic Headspace GC/MS

Introduction The Korean Standard Method for Drinking Water ES 04607.1 requires static headspace with GC/MS to monitor naphthalene. The Minimum Quantitation Limit (MQL) must be less than 3 ppb. ...

ByTeledyne Tekmar


Meeting the Korean Method ES 04601.2 for 1,4-Dioxane with Static Headspace GC/MS

Meeting the Korean Method ES 04601.2 for 1,4-Dioxane with Static Headspace GC/MS

Introduction The Korean Method ES 04601.2 requires static headspace with GC/MS to monitor 1,4-dioxane. The Minimum Quantitation Limit (MQL) must be less than 1 ppb. ...

ByTeledyne Tekmar


Meeting the Korean Method ES 04602.1b for Vinyl Chloride, Acrylonitrile, and Bromoform with Static and Dynamic Headspace GC/MS

Meeting the Korean Method ES 04602.1b for Vinyl Chloride, Acrylonitrile, and Bromoform with Static and Dynamic Headspace GC/MS

Introduction The Korean Method ES 04602.1b requires either static or dynamic headspace with GC/MS to monitor vinyl chloride, acrylonitrile, and bromoform. ...

ByTeledyne Tekmar


Meeting the Korean Method ES 04603.2b for 12 VOC with Static and Dynamic Headspace GC/MS

Meeting the Korean Method ES 04603.2b for 12 VOC with Static and Dynamic Headspace GC/MS

Introduction The Korean Standard Method for Drinking Water ES 04603.2b requires static headspace with GC/MS to monitor 12 Volatile Organic Compounds (VOCs). The Minimum Quantitation Limit (MQL) must be less than 5 ppb. ...

ByTeledyne Tekmar


Blood alcohol content analysis using nitrogen carrier gas

Blood alcohol content analysis using nitrogen carrier gas

Standard headspace systems use nitrogen for vial presurization, with helium typically used for GC carrier gas. ...

ByPEAK Scientific Instruments Ltd


Alcoholic Beverage Fusel Alcohol Testing with Static Headspace

Alcoholic Beverage Fusel Alcohol Testing with Static Headspace

Abstract A static headspace method was developed using Teledyne Tekmar automated headspace vial samplers (Figure 1 and Figure 2) to meet the method requirements of the Alcohol and Tobacco Tax and Trade Bureau of the US Department of the Treasury (TTB) method SSD: TM:2001 for testing fusel alcohols in alcoholic beverages. ...

ByTeledyne Tekmar


Achieving low-level detection of benzene in beverages with an automated headspace vial sampler

Achieving low-level detection of benzene in beverages with an automated headspace vial sampler

Abstract Eight commercially available beverage samples were selected for low-level detection of benzene by static headspace analysis. This study will use the Teledyne Tekmar HT3 Automated Headspace Vial Sampler to analyze parts per trillion (ppt) levels of benzene in beverages. ...

ByTeledyne Tekmar


Methanol in Biodiesel by EN14110 with the HT3 and Versa Automated Headspace Analyzers

Methanol in Biodiesel by EN14110 with the HT3 and Versa Automated Headspace Analyzers

One of these qualifications, methanol content, is determined by EN 141103 , a headspace-gas chromatography method. This application note will present data for two different automated headspace vial samplers to meet the performance criteria outlined in EN Method 14110. ...

ByTeledyne Tekmar


Blood Alcohol Determination with the Teledyne Tekmar HT3 and Young Lin YL6500 Gas Chromatograph

Blood Alcohol Determination with the Teledyne Tekmar HT3 and Young Lin YL6500 Gas Chromatograph

Introduction Police and forensic laboratories around the world routinely use headspace-gas chromatography for volatile components in biological fluids. One of the more common headspace analyses is the determination of blood alcohol in cases involving suspected DUI or OVI. ...

ByTeledyne Tekmar


Residual Solvents Testing per ASTM F1884-04 with the Versa and HT3 Automated Headspace Sampler

Residual Solvents Testing per ASTM F1884-04 with the Versa and HT3 Automated Headspace Sampler

Introduction Police and forensic laboratories around the world routinely use headspace-gas chromatography for volatile components in biological fluids. One of the more common headspace analyses is the determination of blood alcohol in cases involving suspected DUI or OVI. ...

ByTeledyne Tekmar


Alternative Methods to RSK 175 Using Purge and Trap Concentration and Automated Headspace for the Analysis of Dissolved Gases in Drinking Water

Alternative Methods to RSK 175 Using Purge and Trap Concentration and Automated Headspace for the Analysis of Dissolved Gases in Drinking Water

Introduction Police and forensic laboratories around the world routinely use headspace-gas chromatography for volatile components in biological fluids. One of the more common headspace analyses is the determination of blood alcohol in cases involving suspected DUI or OVI. ...

ByTeledyne Tekmar


Increasing sample throughput in method 8260 using the novel oven design of the Clarus 600 GC/MS

Increasing sample throughput in method 8260 using the novel oven design of the Clarus 600 GC/MS

Additionally, the PerkinElmer TurboMatrix™ Headspace Trap sample-introduction technology will keep pace with the GC because of its ability to simultaneously equilibrate up to 12 samples; at the moment the GC becomes ready, the TurboMatrix Headspace Trap initiates the next sample analysis. The analytical standards used in this study were diluted in methanol ...

ByPerkinElmer, Inc.


Determination of VOCs in water using static headspace GC/MS with simultaneous full scan and selective ion recording

Determination of VOCs in water using static headspace GC/MS with simultaneous full scan and selective ion recording

The combination of static headspace sample introduction and gas chromatography/mass spectrometry (HS/GC/MS) provides the analyst with a powerful, fully automated technique for the determination of trace volatile organic compounds (VOCs) in water. Samples may be hermetically sealed in the headspace vial at the point of sampling. This approach ...

ByPerkinElmer, Inc.


VialTweeter at UIS250L - Intensive Sonication of Vials

VialTweeter at UIS250L - Intensive Sonication of Vials

The new Hielscher VialTweeter applies this technology to vials, such as autosampler vials, storage vials and reagent vials without the need to open the cap or any water bath. ...

ByHielscher Ultrasonics GmbH


Performance Testing of Conventional and Innovative Downhole Samplers and Pumps for VOC`s in a Laboratory Monitoring Well

Performance Testing of Conventional and Innovative Downhole Samplers and Pumps for VOC`s in a Laboratory Monitoring Well

These samples were compared against a suite of control samples collected from the bottom of the simulated well by opening a sample port, which allowed water to flow out of the well due to gravity and through stainless steel tubing to an EPA standard 40 ml glass vial. A sampling head allowed the vial to be filled and then flushed with any desired volume of water, ...

BySolinst Canada Ltd.


Performance Testing of Conventional and Innovative Downhole Samplers and Pumps for VOC`s in a Laboratory Monitoring Well

Performance Testing of Conventional and Innovative Downhole Samplers and Pumps for VOC`s in a Laboratory Monitoring Well

These samples were compared against a suite of control samples collected from the bottom of the simulated well by opening a sample port, which allowed water to flow out of the well due to gravity and through stainless steel tubing to an EPA standard 40 ml glass vial. A sampling head allowed the vial to be filled and then flushed with any desired volume of water, ...

BySolinst Canada Ltd.

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