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Preparative Chromatography Articles & Analysis

12 articles found

Translational Development: From Benchside to the Clinic  - Case Study

Translational Development: From Benchside to the Clinic - Case Study

In addition to fume hoods, rotary evaporators, and glassware, we are able to use major equipment including a Bruker Avance 300 MHz NMR spectrometer, Agilent 1100 LCMS, preparative HPLC systems, automatic flash chromatography system, hydrogenator, and ozone ...

ByPAI Life Sciences


Purification of natural products - Case Study

Purification of natural products - Case Study

“Due to its versatility, the PrepChrom C-700 is a valuable instrument in our natural product isolation based research group, where preparative techniques such as column chromatography, flash chromatography and preparative HPLC are used on a daily ...

ByBUCHI


Peptide Separation by CPC Case studies

Peptide Separation by CPC Case studies

Preface Centrifugal Partition Chromatography is a liquid-liquid preparative chromatography technique, which efficiently and economically separates compounds without necessitating solid bulk material. ...

ByRotaChrom Technologies LLC


Improved Analysis of Polyfluorinated Alkyl Substances (PFAS) in Environmental Samples Using Optimized ASTM Method 7968/7979

Improved Analysis of Polyfluorinated Alkyl Substances (PFAS) in Environmental Samples Using Optimized ASTM Method 7968/7979

In the method presented here, direct injection without solid-phase extraction (SPE) allows us to maximize throughput and to minimize background caused by the sample preparation step. We used liquid chromatography with triple-quadrupole mass spectrometry (LC–MS/MS) to analyze the fluorotelomer and unsaturated fluorotelomer acids included in ASTM ...

ByShimadzu Scientific Instruments Inc


Loading capacity of silica flash cartridges

Loading capacity of silica flash cartridges

FlashPure Cartridges Optimizing flash chromatography requires finding the ideal cartridge and conditions for a given sample. ...

ByBUCHI


Some notes about Fats and Oils in Food and about FAME and FAMEWAX

Some notes about Fats and Oils in Food and about FAME and FAMEWAX

For this work, Annika Ostermann compared different derivatization and extraction procedures suitable for the determination of the fatty acid composition in plasma and tissues as fatty acid methyl esters using gas chromatography. Sample preparation and derivatization methods for the analysis of small amounts of tissue and low plasma volumes is more challenging ...

ByRestek Corporation


Method Scaling in Preparative HPLC:  Analytical Method & Preparative Method

Method Scaling in Preparative HPLC: Analytical Method & Preparative Method

” Andy: This is one of the most common things we hear from chemists wanting to do preparative chromatography. We also hear the following question pretty often too: VOC: “I have a good analytical HPLC method, how do I scale it to ...

ByWaters Corporation


In Beverly, the Shoe Fits for Bioanalysis!

In Beverly, the Shoe Fits for Bioanalysis!

This past May, many of the nation’s leading bioanalysts gathered in New England to share ideas and explore the latest advances in mass spectrometry, liquid chromatography, and sample preparation for large molecule quantification. ...

ByWaters Corporation


Leader in sample preparation systems benefits from Axetris MFCs’ high dynamic range - Case Study

Leader in sample preparation systems benefits from Axetris MFCs’ high dynamic range - Case Study

Split ratio flexibility of GC injector increased 30-fold A leading manufacturer of analytical sample preparation systems in gas chromatography (GC) switched to Axetris MFCs - and in doing so, simplified their product range, while offering their customers at least 30 times more flexibility in split ratio. The market-leading dynamic range of Axetris mass flow ...

ByAxetris AG


Bioactive compounds from various plants

Bioactive compounds from various plants

Once an active compound is identifi ed, Ufetree produces a prototype powder product from the fractions of preparative liquid chromatography in mini-scale for quality control and development of scale-up methods for the main production. ...

ByBUCHI


Comparing pesticide residues in Amish and commercially grown strawberries and spinach using QuEChERS, Various dSPE Sorbents, and GC-TOFMS

Comparing pesticide residues in Amish and commercially grown strawberries and spinach using QuEChERS, Various dSPE Sorbents, and GC-TOFMS

We used a QuEChERS-based sample preparation method and gas chromatography-time of flight mass spectrometry (GC-TOFMS) for analyzing pesticides. ...

ByRestek Corporation


Understanding the behaviour of molecular weight fractions of natural organic matter to improve water treatment processes

Understanding the behaviour of molecular weight fractions of natural organic matter to improve water treatment processes

The NOM was fractionated and separated using preparative size exclusion chromatography (SEC) and the fractions were chlorinated in the presence of bromide ion. ...

ByIWA Publishing

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